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University of Silesia in Katowice

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Institute of Materials Engineering

In the laboratory, measurements of positron lifetime in solid materials in solid or powdered form are conducted. Research can be carried out at a wide range of temperatures from 173 K to 573 K and in high vacuum reaching 10⁻⁶ bar. The measurement results provide information on the size and distribution of free volume in polymers, as well as the pore size in microporous materials within the range of rh ≈ 1.5 Å to rh ≈ 100 Å. The research technique also enables the characterization of defect structures, including the detection of crystalline structure defects in metallic materials. The laboratory is also equipped with a scanner for measuring α, β, γ and X-ray radiation levels.

  • Positron lifetime spectrometer with a chamber for temperature-controlled measurements, equipped with a vacuum pump allowing a vacuum level of 10⁻⁶ bar to be achieved. The spectrometer has a time resolution of 240 ps. Measurements are conducted using a radioactive 22Na source.
  • VOLTCRAFT RM-400 radiation scanner with high sensitivity for detecting and measuring α, β, γ and X-ray radiation levels in the dose range from 0.01 mSv/h to 1000 mSv/h, pulse dose rate 0–4000 cpm, 0–400 cps, accumulated dose from 0.001 mSv to 9999 Sv, and accumulated pulse count from 0 to 9999. Device sensitivity in a Co-60 radiation field with an intensity of 1 mSv/h: 108 pulses or 1000 cpm/mR/h — for α radiation from 4 MeV, for β from 0.2 MeV, for γ from 0.02 MeV, and for X-ray radiation from 0.02 MeV.
  • THERMOVAC TM 101 portable vacuum gauge for vacuum measurement in the range from 1200 to 5.0 × 10⁻⁴ mbar.

Lab manager:
Kołodziej Sławomir
Biography
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